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STRUCTURAL STUDIES OF ORGANOBORON COMPOUNDS .55. N,N’-DI-TERT-BUTYL-N,N’-DIHYDROXYPROPANE-1,3-DIAMINE(O-B)ETHOXYDIPHENYLB ORANE2 AND N1,N2-DI-TERT-BUTYL-N1,N2-DIHYDROXY-1-PHENYLPROPANE-1,3-DIAMINE(N2-O-B)H YDROXYDIPHENYLBORANE

TitleSTRUCTURAL STUDIES OF ORGANOBORON COMPOUNDS .55. N,N’-DI-TERT-BUTYL-N,N’-DIHYDROXYPROPANE-1,3-DIAMINE(O-B)ETHOXYDIPHENYLB ORANE2 AND N1,N2-DI-TERT-BUTYL-N1,N2-DIHYDROXY-1-PHENYLPROPANE-1,3-DIAMINE(N2-O-B)H YDROXYDIPHENYLBORANE
Publication TypeJournal Article
Year of Publication1992
AuthorsKliegel, W, Lubkowitz, G, Rettig, SJ, Trotter, J
JournalCanadian Journal of Chemistry-Revue Canadienne De Chimie
Volume70
Pagination2033-2039
Date PublishedJul
Type of ArticleArticle
ISBN Number0008-4042
KeywordsCRYSTAL, MOLECULAR-STRUCTURES
Abstract

{The 1,3-propanediamine derivatives N,N’-di-tert-butyl-N,N’-dihydroxy- 1,3-propanediamine and N,N’-di-tert-butyl-N,N’-dihydroxy-1-phenyl-1,3-propanediamine have been prepared and reacted with oxybis(diphenylborane) to yield, respectively, the crystalline organoboron compounds N,N’-di-tert-butyl-N,N’-dihydroxypropane-1,3-diamine(O-B)ethoxydiphenylb orane, 5a, and N1,N2-di-tert-butyl-N1,N 2-dihydroxy-1-phenylpropane-1,3-diamine(N2-O-B)-hydroxydiphenylborane, 5b. Crystals of 5a are monoclinic, C2/c

URL<Go to ISI>://A1992JU75300023