Title | Synthesis and characterization of AlPO4-36: a novel aluminophosphate molecular sieve with ATS structure |
Publication Type | Journal Article |
Year of Publication | 1999 |
Authors | Zahedi-Niaki, MH, Xu, GY, Meyer, H, Fyfe, CA, Kaliaguine, S |
Journal | Microporous and Mesoporous Materials |
Volume | 32 |
Pagination | 241-250 |
Date Published | Dec |
Type of Article | Article |
ISBN Number | 1387-1811 |
Keywords | ADSORPTION, Al-27 and P-31 MAS NMR, AlPO-36, ATS structure type, FRAMEWORK TOPOLOGY, molecular sieves, scanning electron microscopy, SOLID-STATE NMR, THERMAL-STABILITY, VPI-5, WATER, XPS, XRD |
Abstract | AlPO-36, the parent member of the ATS, molecular sieve structure type, has been synthesized hydrothermally from gels containing only Al and P oxides. Four series of syntheses were carried out to determine the best conditions for the preparation of AlPO-36 free of AlPO-H3, Characterization of the synthesis products was performed using X-ray diffraction (XRD), chemical analysis, scanning electron microscopy (SEM), N-2 adsorption, X-ray photoelectron spectroscopy (XPS) and Al-27 and P-31 MAS NMR. X-ray powder diffraction patterns are comparable to those previously reported for MAPO-36. (C) 1999 Elsevier Science B.V. All rights reserved. |
URL | <Go to ISI>://000083989500002 |