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Triphenylboroxin complex with N-cyclohexylhydroxylamine and its isobutyraldehyde nitrone

TitleTriphenylboroxin complex with N-cyclohexylhydroxylamine and its isobutyraldehyde nitrone
Publication TypeJournal Article
Year of Publication2002
AuthorsKliegel, W, Lubkowitz, G, Patrick, BO, Rettig, SJ, Trotter, J
JournalActa Crystallographica Section E-Structure Reports Online
Volume58
PaginationO1034-O1037
Date PublishedSep
Type of ArticleArticle
ISBN Number1600-5368
KeywordsBORON CHELATE, CRYSTAL, LIGAND, MOLECULAR-STRUCTURES, ORGANOBORON COMPOUNDS, REACTION-PRODUCTS, REARRANGEMENT
Abstract

N-Cyclohexylhydroxylamine(O-B)triphenylboroxin N-cyclohexyl-C-(2-propyl)nitrone hemibenzene hemisolvate, C24H28B3NO4.C10H19NO.0.5C(6)H(6), contains one molecule of N-cyclohexylhydroxylamine in its N-oxide form added to a boroxin heterocycle, with one molecule of N-cyclohexyl-C-(2-propyl)nitrone linked by an O...H-N hydrogen bond to the protonated hydroxylamine moiety, and a molecule of benzene which is located on a centre of inversion.
URL<Go to ISI>://000177736200049